ISIS Neutron and Muon Source Data Journal

Neutron diffraction to investigate thermal Stability of Ni-Based Alloys at Cryogenic and Elevated Temperatures

Abstract: The project examines the high and cryogenic temperature structural response and thermal stability of a thermally sprayed nickel-based high entropy alloy (HEA) coating using advanced neutron diffraction. HEAs, comprising multiple principal elements in near-equiatomic ratios, are a novel class of materials with excellent mechanical and thermal properties. Despite increasing interest in their use as high-performance coatings, their behaviour under extreme conditions, particularly when thermally sprayed, remains poorly understood. This study focuses on a HEA, designed using machine learning and deposited via atmospheric plasma spraying at LSBU. Neutron diffraction lies at the core of the investigation, offering through-thickness insights with resolution and penetration depth not achievable by other techniques. Its ability to probe dense metallic coatings makes it ideal for assessing structural evolution under thermal loading. Comparative analysis of powder and two coated samples, supported by molecular dynamics simulations, will enhance understanding of the material?s performance in service conditions. By addressing key knowledge gaps in complex multi-element systems under non-equilibrium conditions, the project supports the development of more robust coatings for demanding applications. It aligns with UK priorities in digital manufacturing and advanced materials and forms a major part of a PhD thesis focused on intelligent thermal spray systems with embedded sensing.

Public release date: 03 March 2029

Principal Investigator: Miss Beth Irungu
Experimenter: Mr Andrew Stephen Ascroft
Experimenter: Mr Imran Khan
Experimenter: Professor Nadimul Faisal
Experimenter: Professor Saurav Goel
Local Contact: Dr Tung Lik Lee
Experimenter: Dr Nirmal Kumar
Experimenter: Dr Mubarak Abdelrasoul Elnour Ismail

DOI: 10.5286/ISIS.E.RB2520232-2

Parent DOI: 10.5286/ISIS.E.RB2520232

ISIS Experiment Number: RB2520232

Part Number: 2

Date of Experiment: 01 March 2026

Publisher: STFC ISIS Neutron and Muon Source

Data format: RAW/Nexus
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Data Citation

The recommended format for citing this dataset in a research publication is as:
[author], [date], [title], [publisher], [doi]

For Example:
Miss Beth Irungu et al; (2026): Neutron diffraction to investigate thermal Stability of Ni-Based Alloys at Cryogenic and Elevated Temperatures, STFC ISIS Neutron and Muon Source, https://doi.org/10.5286/ISIS.E.RB2520232-2

Data is released under the CC-BY-4.0 license.